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国家自然科学基金(51004011)

作品数:7 被引量:39H指数:4
相关作者:田建军刘华飞李俊王健张深根更多>>
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Recycle of valuable products from oily cold rolling mill sludge被引量:5
2013年
Oily cold rolling mill (CRM) sludge contains lots of iron and alloying elements along with plenty of hazardous organic components, which makes it as an attractive secondary source and an environmental contaminant at the same time. The compound methods of "vacuum distillation + oxidizing roasting" and "vacuum distillation + hydrogen reduction" were employed for the recycle of oily cold rolling mill sludge. First, the sludge was dynamically vacuum distilled in a rotating furnace at 50 r/rain and 600℃ for 3 h, which removed almost hazardous organic components, obtaining 89.2wt% ferrous resultant. Then, high purity ferric oxide powders (99.2wt%) and reduced iron powders (98.9wt%) were obtained when the distillation residues were oxidized and reduced, respectively. The distillation oil can be used for fuel or chemical feedstock, and the distillation gases can be collected and reused as a fuel.
Bo LiuShen-gen ZhangJian-jun TianDe-an PanYang LiuAlex A.Volinsky
关键词:SLUDGERECYCLINGDISTILLATIONOXIDATION
New technology for recycling materials from oily cold rolling mill sludge被引量:3
2013年
Oily cold rolling mill (CRM) sludge is one of metallurgical industry solid wastes. The recycle of these wastes can not only protect the environment but also permit their reutilization. In this research, a new process of "hydrometallurgical treatment + hydrothermal synthesis" was investigated for the combined recovery of iron and organic materials from oily CRM sludge. Hydrometallurgical treatment, mainly including acid leaching, centrifugal separation, neutralization reaction, oxidizing, and preparation of hydrothermal reaction precursor, was first utilized for processing the sludge. Then, micaceous iron oxide (MIO) pigment powders were prepared through hydrothermal reaction of the obtained precursor in alkaline media. The separated organic materials can be used for fuel or chemical feedstock. The quality of the prepared MIO pigments is in accordance with the standards of MIO pigments for paints (ISO 10601-2007). This clean, effective, and economical technology offers a new way to recycle oily CRM sludge.
Bo LiuShen-gen ZhangJian-jun TianDe-an PanLing MengYang Liu
关键词:HYDROMETALLURGY
Electromagnetic and microwave absorbing properties of FeCoB powder composites被引量:7
2013年
The electromagnetic and microwave absorbing properties of FeCoB powder composites prepared by sin- gle-roller melt-spinning and mechanical milling processes were investigated in this paper. The result indicates that the flake-like powders are obtained. As milling time increases, the flake-like powder particles tend to agglomerate, causing the flake-like powders decrease gradually. The milling time plays an important role in the electromagnetic parameters which relates to the shape and size of the powder particles. The calculation shows that the sample milled for 6 h could achieve an optimal reflection loss of -11.5 dB at 5.8 GHz, with mass fraction of 83 % and a matching thickness of 1.8 mm. The result also indicates that the microwave absorbing properties of the FeCoB powder composites are adjustable by changing their thickness, and can be applied as a thinner microwave absorbing material in the range of 2-8 GHz.
Shen-Gen ZhangHang-Xin ZhuJian-Jun TianDe-An PanBo LiuYan-Tao Kang
铁基软磁复合材料成形和热处理工艺研究被引量:11
2011年
采用磷化处理后的还原铁粉,通过压制、热处理获得铁基软磁复合材料(ISMCs),探讨了成形压力和热处理工艺对材料磁导率、磁损耗和频率特性影响。研究结果显示,900 MPa压力获得密度为7.2 g/cm3磁粉芯,振幅磁导率aμ≥100(30~250 kHz),且μa频率稳定性好(变化量≤0.02~0.03/kHz)。经400℃热处理后,aμ超过120(30~250 kHz),提高了20%。热处理温度超过450℃,磁粉芯的磁损耗显著增加、μa急剧下降。损耗分离研究显示,磁损耗增加主要体现在涡流损耗急剧上升。再经TG-DTA分析,磷化铁粉在462℃时出现一个明显的吸热峰,主要是磷酸氢盐发生分解反应,导致绝缘层破坏,进而影响材料的磁性能。
田建军张德金袁勇崔建民李霆
关键词:软磁复合材料磷化磁损耗
Strontium ferrite powders prepared from oily cold rolling mill sludge by solid-state reaction method被引量:4
2013年
Oily cold rolling mill (CRM) sludge is one of the pollutants emitted by iron and steel plants. Recycling oily CRM sludge can not only reduce pollution but also bring social and environmental benefits. In this study, using oily CRM sludge as sources of iron oxide, the strontium ferrite powders were synthesized in multiple steps including vacuum distillation, magnetic separation, oxidizing roasting, and solidstate reaction. The optimal technological conditions of vacuum distillation and oxidizing roasting were studied carefully. To consider the effects of Fe203/ SrCO3 tool ratio, calcination temperature, milling time and calcination time on magnetic properties of prepared strontium ferrite powders, the orthogonal experimental method was adopted. The maximum saturation magneti- zation (62.6 mA-m2.g-1) of the synthesized strontium ferrite powders was achieved at the Fe203/SrCO3 mol ratio of 6, 5 h milling time, 1250 ~C calcination temperature, and 1 h calcination time. Strontium ferrite powders syn- thesis method not only provides a cheap, high quality raw material for the production of strontium ferrite powders, but also effectively prevents the environmental pollution.
Bo LiuShen-Gen ZangJian-jun TianDe-an PanHang-Xin Zhu
关键词:RECYCLING
烘烤硬化钢板的研究进展被引量:9
2013年
概述了烘烤硬化(BH)钢板的分类、烘烤硬化机理和组织性能研究现状等,介绍了BH钢板的生产工艺流程及各工序对烘烤硬化性能的影响,并指出了BH钢板目前研究工作中存在的若干问题和未来发展方向。
邝春福张深根李俊王健刘华飞
关键词:仿真技术
Bonded Terfenol-D composites with low eddy current loss and high magnetostriction被引量:2
2010年
Bonded Terfenol-D composites,with high electrical resistivity and low eddy current loss,can be used in an alternating magnetic field with high frequency.However,the nonmagnetic binder impairs the magnetostriction of the composites.To achieve high magnetostriction and low eddy current loss,the mixture of the alloy powder and binder was compressed at low pressure in an oriented magnetic field.After this,the aligned samples were recompressed by cold isostatic pressing(CIP).Besides,the effect of particle size on the magnetostriction of the bonded Terfenol-D composites was also studied.The results showed that the bonded Terfenol-D composites had excellent magnetostriction when the particle size was 50-80 μm.The oriented magnetic field and CIP could improve the magnetostriction of the bonded composites,which reaches 1020×10-6.The bonded Terfenol-D composites had good compact structure and high density(7.24 g/cm3).The magnetic loss of the bonded Terfenol-D composites was 192 mW/cm3 at a frequency of 100 kHz in a magnetic field of 960 A/m,which was about one third of that of casting Terfenol-D alloys.
TIAN Jianjun,ZUO Zhijun,PAN De’an,and ZHANG Shengen School of Materials Science and Engineering,University of Science and Technology Beijing,Beijing 100083,China
关键词:COMPOSITESTERFENOL-DMAGNETOSTRICTIONDENSITY
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