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周仁杰

作品数:3 被引量:10H指数:2
供职机构:合肥工业大学更多>>
发文基金:国家自然科学基金安徽省自然科学基金更多>>
相关领域:轻工技术与工程医药卫生更多>>

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凹凸棒石负载姜精油复合物的表征及抗菌活性研究
本论文首先研究了姜精油超临界CO2萃取技术提取工艺的优化,通过单因素、响应面优化方法得到了最佳的姜精油提取工艺。然后用活化的凹凸棒石作为载体,结合出一种新型凹凸棒石负载姜精油复合物;并对该复合物的表征开展了研究;最后,通...
周仁杰
关键词:姜精油凹凸棒石抗菌活性分子机理
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Optimization of Supercritical Carbon dioxide Extraction of Ginger Essential Oil by Response Surface Method被引量:5
2016年
[Objective] Ginger essential oil (GEO) is widely used in food production and medical field in recent years due to its prominent biological functions, and this study was conducted to obtain high-quality and high-purity ginger essential oil from the fresh ginger. [Method] GEO was extracted from ginger roots by supercritical fluid extraction (SFE) method. The effects of flow rate of CO2, mesh size of ginger powder and volume of entrainer were investigated by single-factor experiments and response surface method. The content and extraction rate of 6-gingerol represented the extraction index of GEO. [Result] The conditions were optimized as follows: flow rate of CO2 at 25 L/h, mesh size of ginger power of 80 mesh, and volume of anhydrous ethanol as entrainer of 92.46 ml. The optimal extraction rate of 6-gingerol was 3.21%, which was predicted by RSM. [Conclusion] The optimal process of supercritical carbon dioxide extraction of ginger essential oil was identified by singlefactor experiments and response surface method. The present study provides a satisfactory method for purifying GEO from ginger for industrial purpose.
雷红周仁杰魏巧年李晓乐吴静
Optimal Conditions for the Purification of Sesamin by Recrystallization被引量:4
2017年
[Objective] Sesamin has been widely used in healthy food and medicines in recent years due to its prominent biological functions. This study was aimed to determine the optimal parameters for sesamin recrystallization, to obtain high-quality and high-purity sesamin. [Method] The effects of solid-liquid ratio, heating tempera- ture and cooling temperature on sesamin recrystallization were investigated by sin- gle-factor experiments and orthogonal array testing (ORT). The purity of resulting sesamJn was investigated by HPLC, [Result] The optimal conditions for the purifica- tion of sesamin were solid-liquid ratio of 1:10, heating temperature of 45 ℃ and cooling temperature of 25 ℃. Under these conditions, the purity of sesamin reached 95.26%. [Conclusion] Recrystallization is an effective technique to purify sesamin from sesame meal. Moreover, HPLC is also an ideal method for analyzing the purity of sesamin.
刘末周仁杰吴静雷红
关键词:SESAMINRECRYSTALLIZATIONHPLC
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